Laboratory of Electron Microscopy

Employees:

• Ph.D., senior scientist Ye.V. Tatyanin
• Research assistant L.A. Ivanov
• Ph.D., Research assistant I.A. Perezhogin
• Julia S. Buranova
• Alexander N. Semenov

Scientific activity:

Transmission electron microscopy studies by a JEM-2010 device with an EDS attachment (elemental analysis).

DEVELOPMENTS AND ACHIEVEMENTS (FROM 1996). LITERATURE:

• V.Blank, B.A.Kulnitskiy, Crystallogeometry of polymorphous transitions in Si under pressure, High Pressure Research, 1996, 15, 12(31-42)
• V.Blank, B.A.Kulnitskiy, Ye.Tatyanin, New structure after thermobaric treatment of solid C₆₀, Physics letters 1997, A225,27, 4,
• V.D.Blank, B.A.Kulnitskiy, The habit plane of martensite at bcc-hcp phase transformation, Scripta Materialia 1997,37,3, 4(373-376)
• В.Бланк, О.Жигалина, Б.А.Кульницкий, Е.Татьянин, Искажение ГЦК-структуры при термобарической обработке C₆₀ Кристаллография 1997,42,4, 4(645-648)
• V.Blank, B.A.Kulnitskiy, Ye.Tatyanin, O.M.Zhigalina, TEM study of the crystalline and amorpous phases in C₆₀ , Inst. Phys. Conf. Ser. EMAG97, 1997, Cambridge, UK, No 153, Section 13, 4(593-596)
• V.Blank, S.Buga, N.Serebryanaya,G.Dubitskiy, B.N. Mavrin, M.Popov, R.H.Bagramov, V.Prohorov, S.N.Sulyanov, Ye. Tatyanin, B.A.Kulnitskiy, Struct. and phys prop of superhard and ultrahard 3D polimer. fullerit. creat. from sol C₆₀ by high pres high temp treatment. Carbon 1998, 36,5-6 6(665-670)
• V.Blank, B.A.Kulnitskiy, Ye.Tatyanin, O.M.Zhigalina, A new phase of carbon, Carbon, 1999, 37, 4, 6 (549-554)
• V.D.Blank, Ye.V.Polyakov, A.A.Nuzhdin, Yu.L.Alshevskiy, B.A.Kulnitskiy, U.Bangert, A.J.Harvey, H.J.Davock, Nanocarbons formed in a hot isostatic pressure apparatus, Thin solid films 1999, 346 , 5 (86-90)
• V.D.Blank, V.V.Aksenenkov, M.Yu.Popov, S.A.Perfilov, Ye.V.Tatyanin, B.A.Kulnitskiy, O.M.Zhigalina, B.N.Mavrin, V.N.Denisov, A.N.Ivlev, V.M.Chernov, V.A.Stepanov, A new carbon structure formed at MeV neutron Diamond and related materials, 1999, 8, 6(1285-1290)
• VD Blank, B.A.Kulnitskiy, OM Zhigalina, Direct phase transformation from the intermediate carbon phase (ICP) into graphite In. Phys. Conf.Ser. 1999 4(421-424)
• VD Blank, B.A.Kulnitskiy, Polimerisation of C₆₀ and C₇₀ under thermobaric treatment In. Phys. Conf.Ser. 1999 4(425-428)
• VD Blank, B.A.Kulnitskiy, OM Zhigalina, Dimerisation and polimerisation of C₇₀ after thermobaric treatment, Carbon, 2000 4(2051-2054)
  
• Бланк, Нуждин, Аксененков, Белогорохов, Кульницкий, Кленов, Углеродазотные структуры, полученные в газоразрядном процессе, Сверхтвердые материалы, 2000, том 2 , 6 (19-24)
• Бланк, Буга, Дубицкий, Серебряная, Попов, Прохоров, Кульницкий, В.М.Левин, Х-М Жу, Э.Нянчи, Б.Сундквист, А.Франссон, Синтез при высоком давлении, структура и физические свойства сверх- и ультратвердых фуллеритов. Физика и техника высоких давлений, 2000, 10(4), 127-132.
• SG Buga, VD Blank, NR Serebryanaya, B.A.Kulnitskiy, M Klaeser, G.Liu, S Lebedkin, Structure and properties of solid LaC82 endofullerene polimerized under pressure 9.5GPa and tem-re 520-720 K Synthetic metals, 2001, 121, 4(1093-1096)
• 16. A Seepujak, A Gutierrez-Sosa, A J Harvey, U Bangert, V D Blank, B A Kulnitskiy, D V Batov, Correlating low-loss EELS and ELNES of carbon nano-structures, Inst.Phys.Conf.Ser.168, 2001, 4(307-311).
• V.D.Blank, B.A.Kulnitskiy, D.V.Batov, U.Bangert, A.Gutierrez-Sosa, A.J.Harvey, Electron Microscopy and electron energy loss spectroscopy studies of carbon fiber formation at Fe catalysts. Journal of Applied Physics V 91, #3 1 february 2002 4 (1657-1660)
• V.D. Blank, B.A.Kulnitskiy, D.V. Batov, U. Bangert, A. Gutierrez-Sosa, A.J. Harvey, Transmission electron microscopy studies of nanofibers formed on Fe"7C"3-carbide, Diamond and related materials, 2002, V 11 N 3-6 4 (931-934)
• V.D. Blank, B.A.Kulnitskiy, O.M.Zhigalina, Direct phase transformation of the intermediate carbon phase into graphite under electron-beam irradiation. Сверхтвердые материалы, 2002, 4, 3-7.
• Yu.N.Parkhomenko, E.A.Skrileva, B.L.Sanakoev, V.D.Blank, B.A.Kulnitskiy, G.A.Dubitsky, N.R.Serebryanaya, S.G.Buga, Carbon bonds hybridization in fullerites studied by XPS. Nanotechnologies in the area of physics, chemistry and biotechnology, Proceedings. Fifth ISTC Scientific Advisory Committee Seminar, St-Petersburg Russia, May, 27-29, 2002, 333-336.
• V.D. Blank, E.V.Polyakov, B.A.Kulnitskiy, D.V. Batov, U. Bangert, A. Gutierrez-Sosa, A.J. Harvey, A.Seepujak, Formation of N-containing C-nanotubes and nanofibers by carbon resistive heating under high nitrogen pressure, Diamond and related materials, 2003, 12, 864-869.
• V.D. Blank, D.V. Batov, S.G.Buga, B.A.Kulnitskiy, E.V.Polyakov, Sahn Nam, Yun-Hi Lee, U. Bangert, A. Gutierrez-Sosa, A.J. Harvey, A.Seepujak, Yung-Doo Lee, Duck-Jung Lee, Byeong-Kwon Ju, Formation of C-N nanofibers in high isostatic pressure Apparatus and their Field Emission Properties, Proceedings of the Applied Diamond Conference ,Third Frontier Carbon Technology Conference (ADC/FCT2003), 533-538
• V.D. Blank, S.G.Buga, E.V.Polyakov, D.V. Batov, B.A.Kulnitskiy, U. Bangert, A. Gutierrez-Sosa, A.J. Harvey, A.Seepujak, Yung-Doo Lee, Duck-Jung Lee, Byeong-Kwon Ju Structure and field emission of C-N nanofibers, formed in High Isostatic Pressure Apparatus. Proceedings CP685. Molecular Nanostructures: XVII Int. Winterscool/ Euroconference on Electronic Properties of Novel Materiaaals, 2003 AIP, 477-480.
• В.Д.Бланк, А.Н.Кириченко, В.Н.Денисов, Б.А.Кульницкий, К.В.Гоголинский, Н.И.Батова, В.Ф.Кулибаба, С.А.Терентьев. Особенности структурного изменения графита в камере высокого давления с алмазными наковальнями. Сверхтвердые материалы, 2004, 3, 3-11.
• A.Seepujak, U.Bangert, A.Gutierrez-Sosa, A.J.Harvey, A.Papworth, V.D.Blank, B.A.Kulnitskiy, D.V.Batov. Tuning the Energy of split surface electron energy-loss resonances excited on a multi-wall carbon nanotube.Microscopy and Microanalysis. 10 (suppl.2), 2004.
• V.D.Blank, B.A.Kulnitskiy Proposed formation mechanism for helically coiled carbon nanofibers, Carbon, 2004, 42, 3009-3011.
• Seepujak, U. Bangert, A. Guttierrez-Sosa, A.J.Harvey, V.D. Blank, B.A.Kulnitskiy, D.V.Batov, 3D spectrum imaging of multi-wall carbon nanotube coupled π-surface modes utilizing electron energy-loss spectra acquired using a STEM/Enfina system, Ultramicroscopy, 2005, 104, 57-72.
• V.D.Blank, B.A.Kulnitskiy, G.A.Dubitsky, I.Alexandrou, The structuires of C₆₀-phases, formed by thermobaric treatment:HREM studies, Fullerenes, nanotubes and carbon nanostructures, v.13, suppl. 1, 2005, 167-177.
• Д.В.Батов, В.Д.Бланк, Е.В.Поляков, Б.А.Кульницкий, Б.К.Джу, Углерод-азотные нанотрубки, полученные в газостате, и их применение в качестве холодных катодов, Физика и техника высоких давлений, 2005. 15, 2, 47-51.
• A.Seepujak, U.Bangert, A.J.Harvey, V.D.Blank, B.A.Kulnitskiy, D.V.Batov, EEL Calculations and Measurements of Graphite and Graphitic-CNx Core-Losses, In. Phys. Conf.Ser, 26, 2006, 161-164.
• V.D.Blank, Yu.L. Alshevskiy, Yu.A.Belousov, N.V.Kazennov, I.A.Perezhogin, B.A.Kulnitskiy, TEM studies of carbon nanofibres formed on Ni catalyst by bolyethilene pyrolysis, Nanotechnology, 17, 2006, 1862-1866.
• Peculiarities of deformation-induced amorphization in CoZrNi alloys. E.E.Novikova, Ye.V.Tatyanin, V.G.Kurdjumov, Scripta Metallurgica et Materialia, (1995), 851, v.33.
• Е.В.Татьянин, Н.Ф.Боровиков, В.Г.Курдюмов, В.Л.Инденбом, ФТТ, 1997, Аморфные полосы сдвига в деформированном TiNi-сплаве, т.39,стр.1237-1239
• E.A.Ekimov, A.G.Gavriluk, B.Palosz, S.Glerlotka, P.Dluzewski, E.Tatyanin, Yu.Kluev, A.M.Naletov, A.Presz. High - pressure, high temperature synthesis of SiC - diamond ceramics. Applied Phys. Letters, v.77, N7(2000) pp. 954-956.
• S.D.Prokoshkin, I.Yu.Khmelevskaya, S.D.Dobatkin, E.V.Tatyanin, .B.Trubitsyna, V.V.Stolyarov, E.A.Prokofiev, Alloy composition, deformation temperature, pressure and post-deformation annealing effects in severely deformed Ti-Ni based shape memory alloys. Acta Materialia, 53(2005) 2703-2714.
• E.V. Tat’yanin, A.G. Lyapin, V.V.Mukhamadiarov, V. V. Brazhkin and A.L. Vasiliev, Mechanism of formation of the superhard disordered graphite-like phase from fullerite C₆₀ under pressure. J. Phys.: Condens. Matter 17 (2005) 249–256
• V.D.Blank, Yu.L.Alshevskiy, A.I.Zaitsev, N.V.Kazennov, I.A.Perezhogin, B.A.Kulnitskiy, Structure and phase composition of a catalyst for carbon nanofiber formation, Scripta Materialia, 55 (2006) 1035-1038.
• Бланк В. Д., Кульницкий Б. А., Пеpежогин И. А., Альшевский Ю. Л., Батов Д. В., Казеннов Н. В., Нанотpубка как pеакционная ячейка. Дефоpмационные пpоцессы в нанотpубках Материаловедение, 2007, 1, 42-49.
• V.D.Blank, D.V.Batov, B.A.Kulnitskiy, E.V.Polyakov, I.A.Perezhogin, D.A.Podgorny, Yu.N.Parkhomenko, Y-junction bamboo-like CNx nanotubes, Сверхтвердые материалы, 2007,4, 13-19.
• V.D.Blank, A.A.Deribas, B.A.Kulnitskiy, I.A.Perezhogin, A.V.Utkin, The formations of onions at shock-wave loading of graphite, Materials science Forum, v.566, 2008, 357-360.
• V.D. Blank, V N Denisov, A N Kirichenko, B A Kulnitskiy, S Yu Martushov, B N Mavrin, I A Perezhogin, High pressure transformation of single-crystal graphite to form molecular carbon – onions, Institute of Physics Publishing, Nanotechnology, 18, 2007.
• V.D.Blank, A.A.Deribas, N.A.Lvova, R.H.Bagramov, B.A.Kulnitskiy, I.A.Perezhogin, V.M.Prokhorov, V.V.Silvestrov, A.S.Yunoshev, Properties of Si3N4 obtained by shock Synthesis, Materials science Forum, v.566, 2008, 129-134.
• Книга (Book): Carbon Nanotubes and Related Structures, Editor(s) Vladimir Blank and Boris Kulnitskiy, Издательство: Research Signpost, Trivandrum, Kerala, (India), 2008, 150 страниц. В книге две статьи: 1. V.D.Blank, B.A.Kulnitskiy, I.A.Perezhogin, TEM studies of carbon nanostructures, grown on iron catalyst. Crystallography of iron carbides. p.97-120 2. A.Seepujak, U.Bangert, A.J.Harvey, A.Bleloch, V.D.Blank, B.A.Kulnitskiy, D.V.Batov, E.V.Polyakov, Nitrogen doping into carbon nanotubes using electron energy-loss spectroscopy, p.49-67.
• V.D.Blank, B.A.Kulnitskiy, I.A.Perezhogin, Structural peculiarities of carbon onions, formed by four different methods: Onions and diamonds, alternative products of graphite high pressure treatment. Scripta Materialia, 2008, 407-410, November.
• V.D.Blank, B.A.Kulnitskiy, I.A.Perezhogin, Yu.L.Alshevskiy, N.V.Kazennov, Decomposition of Fe5C2 catalyst particles in carbon nanofibers during TEM observation, Science and Technology of Advanced Materials (IOP), 10,2009, 1-4.
• B.Kulnitskiy, I.Perezhogin, V.Blank, Structural peculiarities of fcc and bcc catalyst particles and fillings inside carbon nanotubes ( nanofibers) studied by means of electron microscopy, Physics, chemistry and application of nanostructures, 2009, 184-187. Nanomeeting-2009, Minsk.
• M. Popov, V. Medvedev, V. Blank, V. Denisov, A. Kirichenko, E. Tat’yanin, V. Aksenenkov, S. Perfilov, R. Lomakin, E. D’yakov, V. Zaitsev, Fulleride of aluminum nanoclusters, Journal of applied physics, 108, 094317, 2010.
• M. Popov, S. Buga, P. Vysikaylo, P. Stepanov, V. Skok, V. Medvedev, E. Tatyanin, V. Denisov, A. Kirichenko, V. Aksenenkov, and V. Blank, C60-doping of nanostructured Bi–Sb–Te thermoelectrics, Phys. Status Solidi A 208, No. 12, 2783–2789 (2011)
• R. H. Bagramov, V. D. Blank, N. R. Serebryanaya, G. A. Dubitsky, E. V. Tatyanin, V. V. Aksenenkov, High Pressures Synthesis of Iron Carbide Nanoparticles Covered with Onion-Like Carbon Shells, Fullerenes, Nanotubes, and Carbon Nanostructures, 20: 41–48, 2012.
• B.N. Mavrin, V.N. Denisov, A. Kirichenko, E.V. Tat’yanin, L.A. Ivanov, V.V. Aksenenkov, S.A. Perfilov, R. Lomakin, V.D. Blank, V.V. Medvedev, M.Y. Popov, Cu–C60 nanocomposite with suppressed recrystallization, Appl. Phys. А, Published online 10 august 2011.
• V.D. Blank, A. Seepujak, E.V. Polyakov, D.V. Batov, B.A. Kulnitskiy, Yu.N. Parkhomenko, E.A. Skryleva, U. Bangert, A. Gutiérrez-Sosa and A.J. Harvey, Growth and characterisation of BNC nanostructures, Carbon, 47, 14, nov. 2009, 3167-3174, 2009
• V.D. Blank, B.A. Kulnitskiy, I.A. Perezhogin, E.V. Polyakov and D.V. Batov, HRTEM studies of cobalt-filled carbon nanotubes, Acta Materialia, Pages 1293-1298 58, 4, february, 2010. doi:10.1016/j.actamat.2010.10.033
• Аксененков В.В. Баграмов Р.Х. Бланк В.Д. Денисов В.Н. Дубицкий Г.А., Кульницкий Б.А. Маврин Б.Н. Пережогин И.А. Серебряная Н.Р. Скрылева Е.А., Луковичные структуры углерода: порошки и компакты, Химия и химическая технология, Известия высших учебных заведений, 2010, Т. 53, №. 10 Стр. 49-59.
• Г.А.Дубицкий, Н.Р.Серебряная, В.Д.Бланк, Е.А.Скрылева, Б.А.Кульницкий, Б.Н.Маврин, В.В.Аксененков, Р.Х.Баграмов, В.Н.Денисов, И.А.Пережогин, Влияние высоких давлений и температур на наноуглеродные луковичные структуры: сравнение С С60., Изв. АН, химическая, 3, 404-409, 2011.
• В.Д.Бланк, И.А.Пережогин, Б.А.Кульницкий, Взаимосвязь кристаллографической ориентации каталитичеких наночастиц в углеородных нанотрубках и нановолокнах с их структурой и хиральностью, Известия высших учебных заведений, химия и химическая технология, 2011, 54,7,19-26.
• В.Д.Бланк, И.А.Пережогин, Б.А.Кульницкий, Г.А.Дубицкий, Н.Р.Серебряная, Б.Н.Маврин, В.В.Аксененков, Кириченко А.Н., Кузьмин Н.В., Особенности структуры и колебательных спектров системы алмаз-лонсдейлит, Известия высших учебных заведений, химия и химическая технология, 2011, 54,7,10-13.
• Г.А.Дубицкий, Н.Р.Серебряная, В.Д.Бланк, Е.А.Скрылева, Б.А.Кульницкий, Баграмов Р.Х., Пахомов И.В., Получение углерод-азотных материалов из фуллерита С60, Известия высших учебных заведений, химия и хим. технология, 2011, 54,7,73-79.
• V.D.Blank, B.A.Kulnitskiy, I.A.Perezhogin, V.N.Denisov, Mavrin, Serebryanaya, Dubitsky, Aksenenkov, Kirichenko, Kuzmin, First-principles, UV Raman, X-ray diffraction and TEM study of lattice dynamics of the diamond-lonsdaleite system, Diamond and related materials, 2011, 20, 951-953.
• V.D.Blank, B.A.Kulnitskiy, A.A.Nuzhdin, Diamond and related materials, Lonsdaleite formation in process of reverse phase transition diamond-graphite, 2011,20, 1315-1318.
• Ю.С. Буранова, Изучение нанотрубок с кобальтом в качестве наполнителя методами просвечивающей электронной микроскопии, Труды МФТИ, 2011, т. 3, №3, с. 30 – 41.